Welcome to CS!
My first question would be, what kind of hygrometer are you trying to calibrate? If it's one of those analog needle style, they are notorious for inconsistencies.
Make sure you have a good sealing bag, use two if you have to. Also, using a sandwich size gladloc storage container without the lid, put the MOIST salt, (a 2-liter cap-full should be plenty), and the hygrometer in the container, and seal them up really good. leave it overnight. also, it may not make a huge difference, but put the test in a place that has a steady temperature, like your kitchen pantry. Temp fluctuations can cause inaccurate readings.
good luck, and let us know how it works out!
Dennis~
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